1,2-二溴-1,1,2-三氟乙烷合成路线 (共 10 条)
反应条件
bromine; acetic acid
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 843,848;engl.Ausg.S.863,868
反应条件
bromine T=50°C; Product distribution / selectivity;
参考文献
WO2006/26400 A1, ;
Page/Page column 16 ;
反应条件
bromine in dichloromethane T=20°C; 24 h;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 638, # 3-4 p. 565 - 579
反应条件
hydrogen bromide 0.833333 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1266 - 1271
反应条件
Irradiation (UV/VIS); 20°C, with excess of HBr (5:1 molar ratio);
参考文献
F: PerFHalOrg.SVol.3, 6.2.3.5, page 187 - 208
反应条件
in gas Irradiationpressure dependence of the deuterium fraction, isotopic selectivity; further products: B1, B1'; MechanismProduct distribution;
参考文献
Journal of the Chemical Society, Faraday Transactions, , vol. 89, # 5 p. 771 - 774
参考文献
PCBU SERVICES, INC.; PURDUE RESEARCH FOUNDATION
Patent: WO2006/26400 A1, 2006 ;
Location in patent: Page/Page column 14 ;
参考文献
Swarts
Chem. Zentralbl., 1899 , vol. 70, # II p. 281
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran; ethanol
反应条件
cesium fluoride in ethylene glycol dimethyl ether T=20°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, # 11 p. 2233 - 2236
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2531 - 2535