N1-[4-(三氟甲基0苯基]乙酰氨合成路线 （共 34 条）
反应条件
pyridine T=0 - 20°C; 0.5 h;
参考文献
KOWA COMPANY, LTD.
Patent: US2009/62306 A1, 2009 ;
Location in patent: Page/Page column 29 ;
反应条件
potassium phosphate; copper(l) iodide; C8H16N2O*C2H2O4; potassium iodide in N,N-dimethyl-formamide T=130°C; Goldberg Reaction; Inert atmosphere;
参考文献
Mitra, Aurpon W.; Hansen, Marvin M.; Laurila, Michael E.; Kolis, Stanley P.; Martinelli, Joseph R.
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6580 - 6583
反应条件
silver nitrate; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in water; acetone T=55°C; 1 h; Inert atmosphereSchlenk technique;
参考文献
Mizuta, Satoshi; Stenhagen, Ida S.R.; O'Duill, Miriam; Wolstenhulme, Jamie; Kirjavainen, Anna K.; Forsback, Sarita J.; Tredwell, Matthew; Sandford, Graham; Moore, Peter R.; Huiban, Mickael; Luthra, Sajinder K.; Passchier, Jan; Solin, Olof; Gouverneur, Veronique
Organic Letters, 2013 , vol. 15, # 11 p. 2648 - 2651
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2352
Helvetica Chimica Acta, , vol. 30, p. 107,110
反应条件
tert.-butylhydroperoxide; copper(l) chloride in methanol; dichloromethane; water T=0 - 20°C; 12 h;
参考文献
Ye, Yingda; Kuenzi, Stefan A.; Sanford, Melanie S.
Organic Letters, 2012 , vol. 14, # 19 p. 4979 - 4981,3
Title/Abstract Full Text Show Details
Ye, Yingda; Kuenzi, Stefan A.; Sanford, Melanie S.
Organic Letters, 2012 , vol. 14, # 19 p. 4979 - 4981
反应条件
potassium carbonate in acetone T=0 - 30°C; 11 h;
参考文献
Wang, Gong-Bao; Wang, Lin-Fa; Li, Chao-Zhang; Sun, Jing; Zhou, Guang-Ming; Yang, Da-Cheng
Research on Chemical Intermediates, 2012 , vol. 38, # 1 p. 77 - 89
反应条件
in N,N-dimethyl-formamide T=20°C; 18 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Morimoto, Hiroyuki; Tsubogo, Tetsu; Litvinas, Nichole D.; Hartwig, John F.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 16 p. 3793 - 3798
反应条件
2,6-dimethylpyridine in water; acetonitrile T=80°C; Microwave irradiation;
参考文献
Spiteri, Christian; Moses, John E.
Synlett, 2012 , vol. 23, # 10 art. no. ST-2012-D0154-L, p. 1546 - 1548
反应条件
copper; isopentyl nitrite in acetonitrile T=0 - 15°C; Sandmeyer Reaction; 8 h; Schlenk techniqueInert atmosphere; Time;
参考文献
Dai, Jian-Jun; Fang, Chi; Xiao, Bin; Yi, Jun; Xu, Jun; Liu, Zhao-Jing; Lu, Xi; Liu, Lei; Fu, Yao
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8436 - 8439
反应条件
t-Bu-BippyPhos; [Pd(η3-1-Ph-allyl)(μ-Cl)]2; potassium carbonate in 1,4-dioxane T=90°C; Buchwald-Hartwig Coupling; 18 h; Inert atmosphereGlovebox;
参考文献
Crawford, Sarah M.; Lavery, Christopher B.; Stradiotto, Mark
Chemistry - A European Journal, 2013 , vol. 19, # 49 p. 16760 - 16771
