1 -甲基- 5 -苯基- 1H -吡唑合成路线 （共 40 条）
参考文献
v. Auwers; Ottens
Chemische Berichte, 1925 , vol. 58, p. 2076
参考文献
v. Auwers; Wolter
Justus Liebigs Annalen der Chemie, 1932 , vol. 492, p. 283,291
反应条件
das erhaltene Oel bei der Destillation;
参考文献
v. Auwers; Schmidt
Chemische Berichte, 1925 , vol. 58, p. 537
反应条件
N-bromosuccinmide in acetonitrile T=70°C; 1 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2006/102194 A1, 2006 ;
Location in patent: Page/Page column 181 ;
WO 2006/102194 A1
反应条件
N-bromosuccinmide in acetonitrile T=70°C; 1 h;
参考文献
ELI LILLY AND COMPANY
Patent: WO2006/102194 A1, 2006 ;
Location in patent: Page/Page column 181 ;
WO 2006/102194 A1
反应条件
1: 95 percent / Br2 / CHCl3 / Ambient temperature 2: 1) n-BuLi / 1) ether, hexane, -35 to -30 deg C then RT, 15 h, 2) THF,ether, hexane, -30 to 25 deg C, overnight View Scheme
参考文献
Kano, Kunio; Scarpetti, David; Warner, John C.; Anselme, Jean-Pierre; Springer, James H.; Arison, Byron H.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2211 - 2219
反应条件
in methanol Rearrangement; 2 h; Photolysis;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
反应条件
in methanol Rearrangement; ring cleavage; Photolysis; Quantum yieldKinetics;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
反应条件
in methanol
Rearrangement; 2 h; Photolysis;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
反应条件
in methanol
Rearrangement; ring cleavage; Photolysis; Quantum yieldKinetics;
参考文献
Pavlik, James W.; Kebede, Naod
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8325 - 8334
