5-(2-氯苯基)-2-呋喃甲醛合成路线 （共 11 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; toluene T=120°C; 3 h;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; GATTI, Richard A.; DU, Liutao; DAMOISEAUX, Robert; LAI, Chih-Hung; JUNG, Michael; KU, Jin-Mo; BERTONI, Carmen
Patent: US2013/274283 A1, 2013 ;
Location in patent: Page/Page column 0247 ;
反应条件
1: 2-chloro-aniline With hydrogenchloride; water; sodium nitrite T=0 - 5°C; 2: furfural With ammonium cerium(IV) nitrate in water T=20°C; 7 h;
参考文献
Subrahmanya Bhat; Shivarama Holla
Heterocyclic Communications, 2003 , vol. 9, # 6 p. 625 - 628
反应条件
sodium carbonate; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether T=85°C; Suzuki-Miyaura coupling; 9 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 48 p. 9215 - 9219
反应条件
copper(l) chloride in water T=20°C; Meerwein arylation; 48 h;
参考文献
Paizs, Csaba; Taehtinen, Petri; Lundell, Katri; Poppe, Laszlo; Irimie, Florin-Dan; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2003 , vol. 14, # 13 p. 1895 - 1904
反应条件
borane dimethyl sulfide complex in tetrahydrofuran T=50 - 60°C; 2.5 h; Inert atmosphere;
参考文献
ACS Medicinal Chemistry Letters, , vol. 4, # 5 p. 475 - 480
反应条件
CuCl2·2H2O in water; acetone T=20°C; 12 h;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 61, # 46 p. 10858 - 10863
反应条件
copper dichloride in acetone T=20°C; 12 h;
参考文献
Medicinal Chemistry Research, , vol. 23, # 1 p. 426 - 435
反应条件
1: hydrogenchloride; sodium nitrite / water / 0.17 h / |Cooling with ice 2: borane dimethyl sulfide complex / tetrahydrofuran / 2.5 h / 50 - 60 °C / |Inert atmosphere View Scheme
参考文献
ACS Medicinal Chemistry Letters, , vol. 4, # 5 p. 475 - 480
反应条件
1: hydrogenchloride; sodium nitrite / water / 0.17 h / |Cooling with ice 2: borane dimethyl sulfide complex / tetrahydrofuran / 2.5 h / 50 - 60 °C / |Inert atmosphere View Scheme
参考文献
ACS Medicinal Chemistry Letters, , vol. 4, # 5 p. 475 - 480
反应条件
in acetonitrile 4 h; Irradiation; Yields of byproduct given;
参考文献
D'Auria, Maurizio; Antonioletti, Roberto; Mico, Antonella De; Piancatelli, Giovanni
Heterocycles, 1986 , vol. 24, # 6 p. 1575 - 1578
