2'-甲基-[1,1':4',1'']三联苯合成路线 （共 12 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; water; toluene 22.5 h; RefluxInert atmosphere;
参考文献
Nibbs, Antoinette E.; Baize, Amanda-Lauren; Herter, Rachel M.; Scheidt, Karl A.
Organic Letters, 2009 , vol. 11, # 17 p. 4010 - 4013
反应条件
pentacarbonylmanganese bromide in toluene T=50°C; 24 h; Molecular sieveInert atmosphere;
参考文献
Kuninobu, Yoichiro; Nishi, Mitsumi; Yudha, Salprima S.; Takai, Kazuhiko
Organic Letters, 2008 , vol. 10, # 14 p. 3009 - 3011,3
反应条件
pentacarbonylmanganese bromide; scandium tris(trifluoromethanesulfonate) in water; toluene T=80°C; 24 h; Inert atmosphereMolecular sieve;
参考文献
Kuninobu, Yoichiro; Nishi, Mitsumi; Yudha, Salprima S.; Takai, Kazuhiko
Organic Letters, 2008 , vol. 10, # 14 p. 3009 - 3011,3
反应条件
pentacarbonylmanganese bromide; scandium tris(trifluoromethanesulfonate) in water; toluene T=80°C; 24 h; Inert atmosphere;
参考文献
Kuninobu, Yoichiro; Nishi, Mitsumi; Kawata, Atsushi; Takata, Hisatsugu; Hanatani, Yumi; Salprima Yudha; Iwai, Aya; Takai, Kazuhiko
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 334 - 341
反应条件
potassium tert-butylate in N,N-dimethyl acetamide T=70°C;
参考文献
Garst, Michael E.; Dolby, Lloyd J.; Esfandiari, Shervin; Okrent, Rachel A.; Avey, Alfred A.
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 553 - 556
反应条件
1: LiAlH4 / tetrahydrofuran / Heating 2: H2, aq. HCl / Pd-C View Scheme
参考文献
Carruthers,W. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 76 - 79
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal
参考文献
Carruthers,W. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 76 - 79
反应条件
1: AlCl3 2: Pt-C / Heating View Scheme
参考文献
Sidorova,N.G.; Nikonovich,S.D.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, # 6 p. 1921 - 1926,1900 - 1904
反应条件
2: AlCl3 3: Pt-C / Heating View Scheme
参考文献
Sidorova,N.G.; Nikonovich,S.D.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, # 6 p. 1921 - 1926,1900 - 1904
反应条件
in tetrahydrofuran 1.5 h; Ambient temperatureIrradiation; Title compound not separated from byproducts;
参考文献
Boyatzis, Stamatis; Wilkey, John D.; Schuster, Gary B.
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4537 - 4544
