邻苯二亚胺甲基磷酸二乙酯合成路线 （共 14 条）
参考文献
Gao, Jian; Guo, Yang Hui; Wang, Ya Ping; Wang, Xiang Jing; Xiang, Wen Sheng
Chinese Chemical Letters, 2011 , vol. 22, # 10 p. 1159 - 1162
反应条件
in N,N-dimethyl-formamide T=90°C; 2 h;
参考文献
EP2253621 A1, ;
Page/Page column 24 ;
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 12 h; Heating;
参考文献
Chun; Park; Oh; Hong; Kim
Synthesis, 1994 , # 9 p. 909 - 910
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran 48 h; Ambient temperature;
参考文献
Baraldi, P. G.; Guarneri, M.; Moroder, F.; Pollini, G. P.; Simoni, D.
Synthesis, 1982 , # 8 p. 653 - 655
反应条件
sodium hydride T=30°C;
参考文献
Oesapay, George; Szilagyi, Ildiko; Seres, Jenoe
Tetrahedron, 1987 , vol. 43, # 13 p. 2977 - 2984
反应条件
1: 80 percent / PBr3 / 1 h / 140 °C 2: 81 percent / 1 h / 120 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 35 p. 8177 - 8190
反应条件
T=100°C; 20 h; neat (no solvent);
参考文献
Abdou, Wafaa Mahmoud; Khidre, Rizk E.
Monatshefte fur Chemie, 2010 , vol. 141, # 2 p. 219 - 228
反应条件
1: 71 percent / NEt3 / CH2Cl2 / 6 h / Heating 2: 85 percent / tetrabutylammonium fluoride (TBAF) / tetrahydrofuran / 12 h / Heating View Scheme
参考文献
Synthesis, , # 9 p. 909 - 910
反应条件
1: 1.) sodium hydrogencarbonate, AgNO3, 2.) bromine / 1.) water, 15 min, in the dark, 2.) CCl4, room temperature, 2 h. 2: 47 percent / NaH / 30 °C View Scheme
参考文献
Tetrahedron, , vol. 43, # 13 p. 2977 - 2984
反应条件
hydrazine Multistep reaction;
参考文献
Hirschmann, Ralph; Yager, Kraig M.; Taylor, Carol M.; Moore, William; Sprengeler, Paul A.; Witherington, Jason; Phillips, Barton W.; Smith III, Amos B.
Journal of the American Chemical Society, 1995 , vol. 117, # 23 p. 6370 - 6371
