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| CAS号 : | 5332-26-3 |
精确质量 : | 238.95800 |
| 分子式 : | C9H6BrNO2 |
logP : | 1.57290 |
| 分子量 : | 240.05300 |
PSA : | 37.38000 |
N-溴甲基邻苯二甲酰亚胺 | |
N-(Bromomethyl)phthalimide | |
5332-26-3 | |
C9H6BrNO2 | |
240.05300 | |
37.38000 | |
1.57290 | |
238.95800 |
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白色或灰白色晶体粉末
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1.605
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Stable at room temperature in closed containers under normal storage and handling conditions.
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146.7ºC
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Keep container closed when not in use. Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.
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152-155 °C(lit.)
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1.754 g/cm3
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decomposes
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318.9ºC at 760 mmHg
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29251995
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3
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R36/37/38
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S26-S36-S37/39
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Xi
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29251995. Other imides and their derivatives; salts thereof. General tariff:6.5% |
反应瓶中加入25gN-羟甲基邻苯二甲酰亚胺和250mL氯仿,搅拌成悬浮液,通入溴化氢气体并加热到缓慢回流,0.5h后得到透明液体,继续搅拌到不再吸收吸收溴化氢为止,大约5h后得到橙红色液体。将反应混合液倒出,用温水2×400mL(40℃)洗掉反应液中剩余的溴化氢,溶液由橙色变无色,用无水硫酸镁干燥,蒸去氯仿,得白色固体,干燥,用丙酮重结晶,得针状晶体31g,收率91.5%。 | |
用于农药和医药的中间体 |
