1-苯基-2,4-戊二酮合成路线 （共 16 条）
反应条件
1: With sodium amide in diethyl ether T=-5 - 20°C; RefluxInert atmosphere; 2: With hydrogenchloride in water pH=4 - 5;
参考文献
GLAXOSMITHKLINE LLC; BURGESS, Joelle, Lorraine; DUQUENNE, Celine; KNIGHT, Steven, David; MILLER, William, Henry; NEWLANDER, Kenneth, Allen; VERMA, Sharad, Kumar
Patent: WO2013/173441 A2, 2013 ;
Location in patent: Page/Page column 61 ;
反应条件
sodium in water; acetone
反应条件
methanol; water; oxygen; toluene-4-sulfonic acid; palladium dichloride in N,N-dimethyl acetamide T=80°C; P=4560.31 Torr; 40 h; Autoclave; regioselective reaction;
参考文献
Mitsudome, Takato; Yoshida, Syuhei; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Angewandte Chemie - International Edition, 2013 , vol. 52, # 23 p. 5961 - 5964
Angew. Chem., 2013 , vol. 125, # 23 p. 6077 - 6080,4
反应条件
chromium(VI) oxide; sulfuric acid
参考文献
Journal of the American Chemical Society, , vol. 93, # 1 p. 281 - 282
反应条件
magnesium; benzene T=80 - 85°C;
参考文献
Yakugaku Zasshi, , vol. 59, p. 105,106, 109
Chem.Abstr., , p. 4230
反应条件
1: toluene; acetic acid ester 2: sodium View Scheme
参考文献
Chemische Berichte, , vol. 58, p. 338
反应条件
1: KOH-solution View Scheme
参考文献
Chemische Berichte, , vol. 58, p. 338
反应条件
1: sodium / 0 °C 2: KOH-solution 3: sodium View Scheme
参考文献
Chemische Berichte, , vol. 58, p. 338
参考文献
Chemische Berichte, , vol. 58, p. 338
参考文献
Chemische Berichte, , vol. 58, p. 338
