2,2,6-三甲基四氢吡喃合成路线 (共 11 条)
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in water T=185°C; P=7600 Torr; microwave irradiation;
参考文献
Ishibashi, Kenichi; Takahashi, Masaaki; Yokota, Yutaka; Oshima, Koichiro; Matsubara, Seijiro
Chemistry Letters, 2005 , vol. 34, # 5 p. 664 - 665
反应条件
2-mercapto naphthalene in benzene-d6 T=15°C; 0.0833333 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hartung; Gallou
Journal of Organic Chemistry, 1995 , vol. 60, # 21 p. 6706 - 6716
反应条件
1: 85 percent / LiAlH4 / diethyl ether 2: 84 percent / hydromercuration/reduction View Scheme
参考文献
Law
Journal of the Chemical Society, 1912 , vol. 101, p. 1017
Journal of the Chemical Society, 1912 , vol. 101, p. 1550
反应条件
potassium hydrogensulfate T=140°C; 0.75 h; Yield given;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
alkaline hydrogen peroxide; Re2O7 1) CH2Cl2; Multistep reaction;
参考文献
Tang, Suhan; Kennedy, Robert M.
Tetrahedron Letters, 1992 , vol. 33, # 37 p. 5303 - 5306
反应条件
steam; sulfuric acid
参考文献
Rupe; Schlochoff
Chemische Berichte, 1905 , vol. 38, p. 1504
参考文献
Rupe; Liechtenhan
Chemische Berichte, 1908 , vol. 41, p. 1281
参考文献
Doeuvre
Bulletin de la Societe Chimique de France, 1929 , vol. <4>45, p. 359
参考文献
Rupe; Schlochoff
Chemische Berichte, 1905 , vol. 38, p. 1504
参考文献
Doeuvre
Bulletin de la Societe Chimique de France, 1929 , vol. <4>45, p. 359