1-苯基-4-戊烯-1-酮合成路线 （共 116 条）
反应条件
1: 4-bromo-but-1-ene With magnesium in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
2: benzoyl chloride With copper(l) iodide in tetrahydrofuran
T=-15°C; 3 h; Inert atmosphere;
参考文献
Nicolai, Stefano; Sedigh-Zadeh, Raha; Waser, Jeroime
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3783 - 3801
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in water; benzene
T=20°C; P=34202.3 Torr; 16 h; AutoclaveIrradiation;
参考文献
Sumino, Shuhei; Ui, Takahito; Ryu, Ilhyong
Organic Letters, 2013 , vol. 15, # 12 p. 3142 - 3145
反应条件
C15H17N2Ru(1+)*F6P(1-); sodium t-butanolate in toluene
T=110°C; 17 h; Inert atmosphere;
参考文献
Chang, Xu; Chuan, Low Wei; Yongxin, Li; Pullarkat, Sumod A.
Tetrahedron Letters, 2012 , vol. 53, # 12 p. 1450 - 1455
反应条件
tributyl-amine; palladium diacetate; Trifluoroperazine dihydrochloride in toluene
T=130°C; P=15001.5 Torr; 2 h; Gas phase;
参考文献
Giboulot, Steven; Liron, Frederic; Prestat, Guillaume; Wahl, Benoit; Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre; Poli, Giovanni
Chemical Communications, 2012 , vol. 48, # 47 p. 5889 - 5891
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C;
参考文献
Briggs, Michael E.; Zard, Samir Z.
Synlett, 2005 , # 2 art. no. D30104ST, p. 334 - 336
反应条件
hydrogenchloride in pentane
0.5 h; Ambient temperature;
参考文献
Seebach, Dieter; Pohmakotr, Manat
Tetrahedron, 1981 , vol. 37, # 23 p. 4047 - 4058
反应条件
allyl alcohol; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in methanol
T=90°C; 0.75 h;
参考文献
Giboulot, Steven; Liron, Frederic; Prestat, Guillaume; Wahl, Benoit; Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre; Poli, Giovanni
Chemical Communications, 2012 , vol. 48, # 47 p. 5889 - 5891
反应条件
1: phenyl-(2-trimethylsilanylmethyl-cyclopropyl)-methanone With titanium tetrachloride in dichloromethane
0.5 h;
2: cyclohexanone in dichloromethane
T=-78 - 25°C;
参考文献
Yadav, Veejendra K.; Balamurugan, Rengarajan
Organic Letters, 2003 , vol. 5, # 23 p. 4281 - 4284
反应条件
1: phenyl-(2-trimethylsilanylmethyl-cyclopropyl)-methanone With titanium tetrachloride in dichloromethane
0.5 h;
2: pentan-3-one in dichloromethane
T=-78 - 25°C;
参考文献
Yadav, Veejendra K.; Balamurugan, Rengarajan
Organic Letters, 2003 , vol. 5, # 23 p. 4281 - 4284
反应条件
cyclohexa-1,4-diene; DNP in acetonitrile
T=20°C; 0.5 h; Irradiation;
参考文献
Kitamura, Mitsuru; Mori, Yutaka; Narasaka, Koichi
Tetrahedron Letters, 2005 , vol. 46, # 14 p. 2373 - 2376
