1-(3-溴丙氧基)-3-硝基苯合成路线 （共 5 条）
反应条件
potassium carbonate in acetonitrile 24 h; Inert atmosphereReflux;
参考文献
Kawamoto, Masuki; Shiga, Natsuki; Takaishi, Kazuto; Yamashita, Takashi
Chemical Communications, 2010 , vol. 46, # 44 p. 8344 - 8346
反应条件
di-isopropyl azodicarboxylate; polymer bound triphenylphosphine in tetrahydrofuran T=0 - 20°C; 38 h;
参考文献
ABBOTT LABORATORIES
Patent: WO2009/70516 A1, 2009 ;
Location in patent: Page/Page column 131 ;
反应条件
sodium hydroxide; tetrabutylammomium bromide in toluene 24 h; Heating; Yield given. Yields of byproduct given;
参考文献
Reinholz; Becker; Hagenbruch; Schafer; Schmitt
Synthesis, 1990 , # 11 p. 1069 - 1071
反应条件
1: diluted sulfuric acid 2: sodium ethylate View Scheme
参考文献
Wilson; Adams
Journal of the American Chemical Society, 1923 , vol. 45, p. 538
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Baker,B.R.; Ashton,W.T.
Journal of Medicinal Chemistry, 1970 , vol. 13, # 6 p. 1149 - 1154
