1: para-xylene With n-butyllithium; LiK(OCH2CH2NMe2)2; Mg(OCH2CH2OEt)2 in various solvent(s) T=20°C; Metallation; 0.5 h; 2: ethene in various solvent(s) T=80°C; Alkylation; P=7600.51 Torr; 24 h; Further stages.;
参考文献
Steele, Barry R.; Screttas, Constantinos G.
Journal of the American Chemical Society, 2000 , vol. 122, # 10 p. 2391 - 2392
1: With sulfuric acid in ethanol Elimination; 2: With hydrogen; palladium on activated charcoal in ethyl acetate Elimination; P=2068.65 Torr; 38 h; Further stages.;
参考文献
McQuade, D. Tyler; Kim, Jinsang; Swager, Timothy M.
Journal of the American Chemical Society, 2000 , vol. 122, # 24 p. 5885 - 5886
