1: 79 percent / H2SO4 / Ambient temperature 2: SOCl2 / Heating 3: benzene; diethyl ether / 3 h / 0 - 20 °C 4: aq. NaOH / methanol / 3 h / Ambient temperature View Scheme
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di-tert-butylazodicarboxylate; triphenylphosphine in tetrahydrofuran T=20°C; Mitsunobu reaction; 1 h;
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