O,O′-二乙基二硫代磷酸酯合成路线 (共 159 条)
反应条件
und Erwaermen des Reaktionsprodukts mit methanol.Natriummethylat;
参考文献
Bacon; LeSuer
Journal of the American Chemical Society, 1954 , vol. 76, p. 670,671,674
参考文献
Bachinskii,T.P.; Zemlyanskii,N.I.
J. Gen. Chem. USSR (Engl. Transl.), 1968 , vol. 38, p. 2085 - 2087,2019 - 2021
反应条件
triethylamine in dichloromethane 1.) 20 deg C, 0.5 h; 2.) 20 deg C, 3 h; Yield given;
参考文献
Yousif, N. M.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 46, p. 79 - 82
反应条件
(i) aq. H2SO4, (ii) /BRN= 1209228/; Multistep reaction;
参考文献
Ruefenacht,K.
Helvetica Chimica Acta, 1974 , vol. 57, p. 1658 - 1675
反应条件
in benzene T=50°C; 6 h; Mechanism;
参考文献
Mlotkowska, B.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 3 p. 380 - 386
反应条件
P=15 Torr; 8 h; Further byproducts given;
参考文献
Ofitserov, E. N.; Sinyashin, O. G.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 4 p. 738 - 745,602 - 608
反应条件
Ambient temperaturesealed amp.; Product distributionMechanism;
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 371 - 378
反应条件
sodium carbonate in hexane; dichloromethane; water
参考文献
Diamond Shamrock Corporation
Patent: US4238424 A1, 1980 ;
反应条件
sodium carbonate in N,N-dimethyl-formamide T=48°C; 22 h; Heating;
参考文献
Brand, William W.; Carr, Michael C.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 11, p. 323 - 324
参考文献
Diveley et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 139,143