1: NaOH / diethyl ether / 4 h 2: H2SO4 / aq. ethanol / 2 h 3: 94 percent / CaCl2 / 72 h / Ambient temperature View Scheme
参考文献
Landor, Stephen R.; Landor, Phyllis, D.; Kalli, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2921 - 2926
1: 24 percent / SeO2 / dioxane / 2 h / Heating 2: 94 percent / CaCl2 / 72 h / Ambient temperature View Scheme
参考文献
Landor, Stephen R.; Landor, Phyllis, D.; Kalli, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2921 - 2926
Yanovskaya,L.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 774 - 780
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , p. 857 - 865
Landor, Stephen R.; Landor, Phyllis, D.; Kalli, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2921 - 2926
sulfuric acid 24 h; Heating; Title compound not separated from byproducts;
参考文献
Landor, Stephen R.; Landor, Phyllis, D.; Kalli, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2921 - 2926
1: 1.) NaH / 1.) DMSO, 2.) 2 h
2: 93 percent / H2SO4 / H2O / 3 h
3: 52 percent / conc. HCl / diethyl ether / 6 h / 0 °C
View Scheme
参考文献
Landor, Stephen R.; Landor, Phyllis, D.; Kalli, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2921 - 2926
