2-氯-N-羟基苯甲酰胺合成路线 (共 21 条)
反应条件
1: hydroxylamine hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C 2: N-chloro-succinimide / N,N-dimethyl-formamide / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 31 p. 4001 - 4004
反应条件
hydrogenchloride; oxone in N,N-dimethyl-formamide 8 h; Ambient temperature;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Journal of Organic Chemistry, 1992 , vol. 57, # 24 p. 6649 - 6650
反应条件
N-chloro-succinimide in dichloromethane
参考文献
Synthesis, , # 12 p. 1663 - 1668
反应条件
potassium hydrogencarbonate; copper(II) sulfate; sodium L-ascorbate in water; tert-butyl alcohol T=20°C; 1.5 h;
参考文献
Wang, Xi-Zhao; Jia, Jiong; Zhang, Yan; Xu, Wei-Ren; Liu, Wei; Shi, Fang-Niu; Wang, Jian-Wu
Journal of the Chinese Chemical Society, 2007 , vol. 54, # 3 p. 643 - 652
反应条件
(i) Na, MeOH, (ii) /BRN= 2502600/; Multistep reaction;
参考文献
Ramana, P. Venkata; Reddy, A. Ram
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 3 p. 621 - 627
反应条件
triethylamine in water; 1,2-dichloro-ethane; isopropyl alcohol T=-5 - 20°C; Substitution; 4 h;
参考文献
Ma, Jun-An; Ma, Zhi-Hua; Ma, Hong-Min; Huang, Run-Qiu; Shao, Rui-Lian
Synthetic Communications, 2000 , vol. 30, # 9 p. 1563 - 1567
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Das, Sushanta K.; Balasubrahmanyam, S. N.
Journal of Organic Chemistry, 1983 , vol. 48, # 23 p. 4232 - 4236
反应条件
triethylamine; thiourea in tetrahydrofuran Ambient temperature;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Tetrahedron Letters, 1993 , vol. 34, # 51 p. 8283 - 8284
反应条件
triethylamine in tetrahydrofuran Ambient temperature; Yield given;
参考文献
Kim, Jae Nyoung; Jung, Keum Shin; Lee, Hong Jung; Son, Ji Suk
Tetrahedron Letters, 1997 , vol. 38, # 9 p. 1597 - 1598
参考文献
Hussein, Ahmed Q.; El-Abadelah, Mustafa M.; Sabri, Wail S.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 301 - 304