3,7-二甲基-6-辛烯-1-炔基-3-醇合成路线 （共 58 条）
反应条件
ammonia; potassium hydroxide in water T=30°C; P=12076.2 Torr; 5 h;
参考文献
DSM IP Assets B.V.
Patent: EP1852410 A1, 2007 ;
Location in patent: Page/Page column 5 ;
反应条件
in tetrahydrofuran T=0°C; 1 h;
参考文献
Trost, Barry M.; Toste, F. Dean
Journal of the American Chemical Society, 2002 , vol. 124, # 18 p. 5025 - 5036
反应条件
potassium hydroxide in ammonia; water T=30°C; P=12076.2 Torr; 0.0833333 - 5 h;
参考文献
DSM IP ASSETS B.V.
Patent: WO2004/18400 A1, 2004 ;
Location in patent: Page 5-6 ;
反应条件
methanol; sodium methylate T=20°C; 48.25 h;
参考文献
SYMRISE GmbH and Co., KG
Patent: US2009/92725 A1, 2009 ;
Location in patent: Page/Page column 12 ;
参考文献
Rajaram, J.; Narula, A. P. S.; Chawla, H. P. S.; Dev, Sukh
Tetrahedron, 1983 , vol. 39, # 13 p. 2315 - 2322
参考文献
Samochwalow et al.
Doklady Akademii Nauk SSSR, 1956 , vol. 107, p. 103
Doklady Chemistry, 106-111<1956>151
Full Text Show Details
Samochwalow et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2501,2505; engl. Ausg. S. 2560, 2563
参考文献
Ruzicka; Fornasir
Helvetica Chimica Acta, 1919 , vol. 2, p. 184
反应条件
1: palladium/calcium carbonate / Hydrogenation 2: aluminium tert-butylate View Scheme
参考文献
Kimel et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1611,1613
反应条件
sulfuric acid; hydrogen fluoride; trifluoroacetic acid 1) SO2FCl, SbF5, -60 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gavrilyuk, O. A.; Korchagina, D. V.; Osadchii, S. A.; Barkhash, V. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 871 - 885
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 966 - 982
反应条件
epoxysulfonyl fluoride; trifluoroacetic acid 1) SO2FCl, SbF5, -50 deg C, 2) SO2FCl, ether; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gavrilyuk, O. A.; Korchagina, D. V.; Osadchii, S. A.; Barkhash, V. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 871 - 885
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 966 - 982
