反应条件
in diethyl ether byproducts: LiCl; inert atm., Schlenk technique; soln. of Zr-complex in ether cooled (-78°C), dropwise addn. of Li-salt in ether, warmed (over 12 h to ambient temp. with stirring); evapn., extn. (CHCl3), filtration, evapn. (brownish solid), mixt. not further purified; elem. anal., IR;;
参考文献
Organometallics, , vol. 11, p. 1646 - 1655
