N-苯基哌啶-1-硫代甲酰胺合成路线 (共 11 条)
反应条件
in neat (no solvent) T=25°C; 0.166667 h; Milling;
参考文献
Strukil, Vjekoslav; Igrc, Marina D.; Fabian, Laszlo; Eckert-Maksic, Mirjana; Childs, Scott L.; Reid, David G.; Duer, Melinda J.; Halasz, Ivan; Mottillo, Cristina; Friscic, Tomislav
Green Chemistry, 2012 , vol. 14, # 9 p. 2462 - 2473
反应条件
1: piperidine; carbon disulfide With triethylamine in acetonitrile T=0 - 20°C; 0.416667 h; 2: aniline in acetonitrile T=80°C; 6 h;
参考文献
Varun, Begur Vasanthkumar; Prabhu, Kandikere Ramaiah
RSC Advances, 2013 , vol. 3, # 9 p. 3079 - 3087
反应条件
1.1: dichloromethane / 0.17 h / 0 °C 1.2: 1 h / 20 °C 1.3: 2 h 2.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C View Scheme
参考文献
Fromm
Chemische Berichte, 1909 , vol. 42, p. 1954
反应条件
in N,N-dimethyl-formamide 2 h; Heating;
参考文献
Ramadas; Srinivasan
Synthetic Communications, 1995 , vol. 25, # 21 p. 3381 - 3387
参考文献
Gebhardt
Chemische Berichte, 1884 , vol. 17, p. 3039
参考文献
Gebhardt
Chemische Berichte, 1884 , vol. 17, p. 3039
反应条件
anhydrous iron chloride in acetonitrile 6 h; Reflux;
参考文献
Sahoo, Santosh K.; Chakraborty, Supratim; Patel, Bhisma K.
Journal of Sulfur Chemistry, 2012 , vol. 33, # 2 p. 143 - 153
反应条件
anhydrous iron chloride in acetonitrile
6.5 h; Reflux;
参考文献
Sahoo, Santosh K.; Chakraborty, Supratim; Patel, Bhisma K.
Journal of Sulfur Chemistry, 2012 , vol. 33, # 2 p. 143 - 153
反应条件
thiophosgene in water; acetone
Ambient temperature;
参考文献
Abuzar, Syed; Sharma, Satyavan; Iyer, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 3 p. 211 - 212
反应条件
oxygen; copper(II) bis(trifluoromethanesulfonate) in toluene
12 h; Reflux;
参考文献
Banerjee, Arghya; Santra, Sourav Kumar; Rout, Saroj Kumar; Patel, Bhisma K.
Tetrahedron, 2013 , vol. 69, # 43 p. 9096 - 9104