2-(丙烷-2-基)环戊酮合成路线 （共 21 条）
反应条件
sodium hydroxide; dihydrogen peroxide in methanol Ambient temperatureovernight;
参考文献
Berthelot; Vaccher; Devergnies; Flourquet; Debaert
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 5 p. 1525 - 1529
反应条件
bei der Ozonspaltung;
参考文献
Kon; Nutland
Journal of the Chemical Society, 1926 , p. 3108
反应条件
1: 28 percent / 4 N aq. NaOH, H2O2 / methanol / Ambient temperature; overnight 2: 74 percent / conc. H2SO4, HCl(g) / 12 h / Heating View Scheme
参考文献
Berthelot; Vaccher; Devergnies; Flourquet; Debaert
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 5 p. 1525 - 1529
反应条件
sodium hydroxide; dihydrogen peroxide T=-10°C;
参考文献
Le Guillanton,G.
Bulletin de la Societe Chimique de France, 1969 , p. 2871 - 2875
反应条件
lithium salt of 2-nitropropane in N,N,N',N',N'',N''-hexamethylphosphoric triamide
5 h; Ambient temperatureIrradiation;
参考文献
Tamura, Rui; Nakatsuka, Tamon; Ono, Noboru; Kaji, Aritsune
Chemistry Letters, 1980 , p. 281 - 282
反应条件
sodium hydroxide in water; acetone
参考文献
University of Pittsburgh
Patent: US5250735 A1, 1993 ;
反应条件
sodium hydroxide
Ambient temperatureovernight;
参考文献
Berthelot; Vaccher; Devergnies; Flourquet; Debaert
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 5 p. 1525 - 1529
反应条件
1: 1.) t-BuOK / 1.) Me2SO, room temp., 2.) Me2SO, irradiation, room temp., 1.5 h
2: 78 percent / lithium salt of 2-nitropropane / hexamethylphosphoric acid triamide / 5 h / Ambient temperature; Irradiation
View Scheme
参考文献
Ono, Noboru; Tamura, Rui; Eto, Hiromichi; Hamamoto, Isami; Nakatsuka, Tamon; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3678 - 3684
反应条件
hydrogenchloride; zinc(II) chloride
1.) ethyl acetate, room temp.; Yield given. Multistep reaction;
参考文献
Makin, S. M.; Kruglikova, R. I.; Tagirov, T. K.; Kharitonova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1075 - 1078
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1182 - 1185
反应条件
zinc(II) chloride in ethyl acetate
Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Makin, S. M.; Kruglikova, R. I.; Tagirov, T. K.; Kharitonova, O. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 6 p. 1075 - 1078
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 6 p. 1182 - 1185
