3,4-戊二烯-1-炔-1-基苯合成路线 (共 8 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
参考文献
Ruitenberg, K.; Kleijn, H.; Westmijze, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 11 p. 405 - 409
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
参考文献
Ruitenberg, K.; Kleijn, H.; Elsevier, C. J.; Meijer, J.; Vermeer, P.
Tetrahedron Letters, 1981 , vol. 22, # 15 p. 1451 - 1452
反应条件
((trimethylsilyl)methyl)titanocene chloride 1.) THF, -40 deg C to 0 deg C, 1.5 h, 2.) room temperature; Yield given. Multistep reaction;
参考文献
Petasis, Nicos A.; Hu, Yong-Han
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 782 - 783
反应条件
n-butyllithium; copper(I) bromide Yield given. Multistep reaction;
参考文献
Ruitenberg, K.; Meijer, J.; Bullee, R. J.; Vermeer, P.
Journal of Organometallic Chemistry, 1981 , vol. 217, # 2 p. 267 - 271
参考文献
Libman, N. M.; Dmitrieva, T. L.; Kuznetsov, S. G.; Andreev, A. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 231 - 241
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 2 p. 261 - 273
反应条件
hydrazine hydrate T=40 - 50°C; 0.5 h;
参考文献
Khrimyan, A. P.; Karapetyan, A. V.; Badanyan, Sh. O.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 2 p. 189 - 196
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 2 p. 230 - 238
反应条件
in ammonia
refrigerator, several weeks;
参考文献
Libman, N. M.; Dmitrieva, T. L.; Kuznetsov, S. G.; Andreev, A. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 231 - 241
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 2 p. 261 - 273
反应条件
in tetrahydrofuran
T=45 - 50°C; 5 h; Yield given. Title compound not separated from byproducts;
参考文献
Khrimyan, A. P.; Karapetyan, A. V.; Badanyan, Sh. O.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 2 p. 189 - 196
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 2 p. 230 - 238