N-苯基-4,5-二氢恶唑-2-胺合成路线 (共 9 条)
反应条件
tetrachloromethane; triethylamine; triphenylphosphine in pyridine; acetonitrile T=2°C; 20 h;
参考文献
Vorbruggen; Krolikiewicz
Tetrahedron, 1993 , vol. 49, # 41 p. 9353 - 9372
反应条件
KO2 in acetonitrile T=20°C; 10 h;
参考文献
Kim, Yong Il; Kim, Yong Hae
Synlett, 1997 , vol. 1997, # 11 p. 1324 - 1326
反应条件
SiO2*KF in acetonitrile Heating;
参考文献
Fortin, Jessica S.; Cote, Marie-France; Lacroix, Jacques; Desjardins, Michel; Petitclerc, Eric; C.-Gaudreault, Rene
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 15 p. 7277 - 7290
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran T=20°C; Mitsunobu reaction; 0.583333 h;
参考文献
Kim, Taek Hyeon; Lee, Gue-Jae; Cha, Mi-Hyun
Synthetic Communications, 1999 , vol. 29, # 16 p. 2753 - 2758
反应条件
in 1,4-dioxane T=101°C; 7 h;
参考文献
Katritzky, Alan R.; Langthorne, Roland T.; Patel, Ranjan C.; Lhommet, Gerard
Tetrahedron, 1981 , vol. 37, p. 2383 - 2390
反应条件
1: tetrahydrofuran / 20 °C 2: 1 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 0.58 h / 20 °C View Scheme
参考文献
Menne
Chemische Berichte, 1900 , vol. 33, p. 662
参考文献
Menne
Chemische Berichte, 1900 , vol. 33, p. 662
参考文献
Chem. Fabr. v. Heyden
Patent: DE694133 , 1938 ;
DRP/DRBP Org.Chem.
反应条件
T=50°C; Solvolyse; Rate constant;
参考文献
Scott et al.
Experientia, 1957 , vol. 13, p. 183