(Z)-1-偶氮基丙-1-烯-2-醇合成路线 (共 62 条)
反应条件
dirhodium tetraacetate in dichloromethane T=20°C; 12 h; Kinetics; Further Variations:Reagents;
参考文献
Qu, Zhaohui; Shi, Weifeng; Wang, Jianbo
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 217 - 219
反应条件
dirhodium tetraacetate in dichloromethane T=20°C; 12 h; Kinetics; Further Variations:Reagents;
参考文献
Qu, Zhaohui; Shi, Weifeng; Wang, Jianbo
Journal of Organic Chemistry, 2004 , vol. 69, # 1 p. 217 - 219
反应条件
[(η5-C5H5)Ru(PPh3)2Cl] in chloroform-d1 T=60°C; Decomposition; cross coupling;
参考文献
Zotto, Alessandro Del; Baratta, Walter; Verardo, Giancarlo; Rigo, Pierluigi
European Journal of Organic Chemistry, 2000 , # 15 p. 2795 - 2802
反应条件
(i) tBuOCl, EtOH, (ii) aq. H2SO4; Multistep reaction;
参考文献
Baganz,H.; May,H.-J.
Chemische Berichte, 1966 , vol. 99, p. 3766 - 3770
反应条件
1: potassium dimethoxy(phenyl)(trifluoromethyl)borate With chloro-trimethyl-silane in ethylene glycol dimethyl ether T=-20 - -10°C; 0.333333 h; Inert atmosphere; 2: 1-Diazopropan-2-one With methanol in ethylene glycol dimethyl ether T=-20 - 20°C; 3 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 41 p. 5259 - 5263
反应条件
rhodium trifluoroacetate 1 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 8 p. 491 - 492
参考文献
Fridman,A.L. et al.
Zhurnal Organicheskoi Khimii, 1973 , vol. 9, p. 1678 - 1682,1701 - 1704
反应条件
hydrogenchloride; diethyl ether
参考文献
Van Atta et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 1185
反应条件
oxalyl dichloride in dichloromethane 1 h; Ambient temperature;
参考文献
Helvetica Chimica Acta, , vol. 80, # 3 p. 960 - 965
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in dichloromethane 1 h; Ambient temperature;
参考文献
Helvetica Chimica Acta, , vol. 80, # 3 p. 960 - 965