反应条件
in toluene (N2); stirring a soln. of titanium complex and phosphite in toluene at 60°C for 1 h, cooling to 25°C; evapn., dissolving in pentane, filtration through Kieselgur, concn., crystn. at -30°C, column chromy. (SiO2, -20°C, n-pentane, then n-pentane/toluene 1.1, then n-pentane/CH2Cl2 1:1, then CH2Cl2);
参考文献
Meichel, E.; Stein, Th.; Kralik, J.; Rheinwald, G.; Lang, H.
Journal of Organometallic Chemistry, 2002 , vol. 649, # 2 p. 191 - 198