N,O-双(三甲基硅烷基)三氟乙酰胺合成路线 (共 118 条)
反应条件
chloro-trimethyl-silane
参考文献
Svendsen, John S.; Whist, Jon E.; Sydnes, Leiv K.
Organic Mass Spectrometry, 1987 , vol. 22, p. 486 - 492
参考文献
Kliger, G. A.; Lesik, O. A.; Ryzhikov, V. P.; Gleb, L. S.; Loktev, S. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 12 p. 2644 - 2645
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 12 p. 2847 - 2849
参考文献
Siddiqui; Driscoll; Marquez; Roth; Shirasaka; Mitsuya; Barchi Jr.; Kelley
Journal of Medicinal Chemistry, 1992 , vol. 35, # 12 p. 2195 - 2201
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
in acetonitrile RefluxInert atmosphere;
参考文献
Muhammad, Sohail; Bassindale, Alan R.; Taylor, Peter G.; Male, Louise; Coles, Simon J.; Hursthouse, Michael B.
Organometallics, 2011 , vol. 30, # 3 p. 564 - 571
反应条件
1: 1-(4-ethoxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)-propane-1,3-diol With water; oxygen; α,α'-azodiizobutyramidine-dihydrochloride in acetone T=60°C; pH=5; 3 h; Sodium acetate buffer; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With pyridine T=60°C; 1 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 7 p. 2481 - 2491
反应条件
1: 1-(4-ethoxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)-propane-1,3-diol With water; α,α'-azodiizobutyramidine-dihydrochloride in acetone T=60°C; pH=5; 3 h; Inert atmosphereSodium acetate buffer; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With pyridine T=60°C; 1 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 7 p. 2481 - 2491
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
water gas-phase reaction; Product distribution;
参考文献
Gold, Avram; Utterback, David F.; Millington, David S.
Analytical Chemistry, 1984 , vol. 56, p. 2879 - 2882
反应条件
pyridine 0.0833333 h;
参考文献
Mulder, Peter; Louw, Robert
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 10 p. 282 - 287