N,N-二甲基-1-苯乙胺合成路线 (共 30 条)
反应条件
1: With hydrogenchloride in methanol T=20°C; 2: With N-methylpiperidine zinc borohydride in methanol T=20°C; 0.25 h;
参考文献
Alinezhad, Heshmatollah; Tajbakhsh, Mahmood; Zamani, Reza
Synthetic Communications, 2006 , vol. 36, # 23 p. 3609 - 3615
反应条件
1: With titanium(IV) isopropylate in methanol T=20°C; Addition; 2: With sodium tetrahydroborate in methanol T=20°C; Reduction; 1.5 h;
参考文献
Bhattacharyya, Sukanta
Synthetic Communications, 2000 , vol. 30, # 11 p. 2001 - 2008
反应条件
titanium tetrachloride in dichloromethane T=20°C; 36 h;
参考文献
Miura; Ootsuka; Suda; Nishikori; Hosomi
Synlett, 2001 , # 10 p. 1617 - 1619
反应条件
titanium(IV) isopropylate; chloro-trimethyl-silane in tetrahydrofuran T=20°C; 1 h;
参考文献
Tomashenko, Olesya; Sokolov, Viktor; Tomashevskiy, Alexander; Buchholz, Herwig A.; Welz-Biermann, Urs; Chaplinski, Vladimir; De Meijere, Armin
European Journal of Organic Chemistry, 2008 , # 30 p. 5107 - 5111
反应条件
formic acid; magnesium chloride T=175°C;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1587
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether T=-78 - 20°C; 1 h; 2: dimethyl zinc in diethyl ether T=0 - 20°C; 6 h;
参考文献
Murai, Toshiaki; Matsushita, Koji
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 5 p. 1094 - 1103
参考文献
Journal of the American Chemical Society, , vol. 72, p. 2510,2514
反应条件
[Ir(η5-C5Me5)(C6H4-2-C3H5N2)(NCCH3)](PF6) in N-dodecane; toluene T=100°C; 16 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 46 p. 12780 - 12790
反应条件
γ-Al2O3 in gaseous matrix T=250°C; Yield givenYields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 40, # 19 p. 3689 - 3592
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether T=-78 - 20°C; 1 h; 2: dimethyl zinc in diethyl ether T=0 - 20°C; 6 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 186, # 5 p. 1094 - 1103