1: EtCOSEt With lithium diisopropyl amide in dichloromethane T=-78°C; 0.25 h; 2: chloro-trimethyl-silane in tetrahydrofuran T=-78 - 20°C; 2 h; Title compound not separated from byproducts;
参考文献
DeRoy, Patrick L.; Charette, Andre B.
Organic Letters, 2003 , vol. 5, # 22 p. 4163 - 4165
in toluene
addn. of EtC(O)Co(CO)4 soln. to EtSCo(CO)4 soln., -40°C; stirring, -40°C, 30 min; allowing to warm up to +40°C; stirring, 40°C, 2h; detn. by GC-MS;
参考文献
Tasi, M.; Zani, P.; Maccagnani, G.; Palyi, G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1990 , vol. 581, p. 82 - 88
