6,6-二氯双环[3.1.0]己烷合成路线 (共 9 条)
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran; 1,2-dichloro-ethane T=0°C;
参考文献
Chien, Ching-Ting; Tsai, Chia-Chung; Tsai, Chi-Hui; Chang, Tsai-Yuan; Tsai, Ping-Kuei; Wang, Ying-Chuan; Yan, Tu-Hsin
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4324 - 4327
反应条件
tetrabutyl-ammonium chloride in acetonitrile-D3 T=25°C; 168000 h;
参考文献
Chu, Gaosheng; Moss, Robert A.; Sauers, Ronald R.
Journal of the American Chemical Society, 2005 , vol. 127, # 41 p. 14206 - 14207
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride 0.75 h;
参考文献
Ahra, M.; Grignon-Dubois, M.; Dunogues, J.
Journal of Organometallic Chemistry, 1984 , vol. 271, # 1-3 p. 15 - 22
反应条件
(i) NaOPh, (ii) (reduction); Multistep reaction;
参考文献
Robinson,G.C.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3218 - 3222
反应条件
potassium tert-butylate in dimethyl sulfoxide other dichlorocyclopropanes;
参考文献
Journal of Organic Chemistry, , vol. 57, # 15 p. 4080 - 4083
反应条件
(i) NaOPh, (ii) (reduction); Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 32, p. 3218 - 3222
反应条件
lithium in tetrahydrofuran
T=0 - 10°C;
参考文献
Laguerre, Michel; Grignon-Dubois, Micheline; Dunogues, Jacques
Tetrahedron, 1981 , vol. 37, p. 1161 - 1169
参考文献
Bottini,A.T. et al.
Tetrahedron, 1972 , vol. 28, p. 4701 - 4710
反应条件
aluminium trichloride in carbon disulfide
T=-5°C;
参考文献
Reinhard,D.; Weyerstahl,P.
Chemische Berichte, 1977 , vol. 110, p. 138 - 145