N-(己烷-2-亚基氨基)-2,4-二硝基苯胺合成路线 （共 15 条）
反应条件
1: water; H3PO4-kieselguhr / 204 °C View Scheme
参考文献
Schaad; Ipatieff
Journal of the American Chemical Society, 1940 , vol. 62, p. 179
参考文献
Bowden; Jones
Journal of the Chemical Society, 1946 , p. 52
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Heilbron et al.
Journal of the Chemical Society, 1945 , p. 84,87
Journal of the Chemical Society, 1947 , p. 1586,1588
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Henne; Hill
Journal of the American Chemical Society, 1943 , vol. 65, p. 753
Full Text Show Details
Schaad; Ipatieff
Journal of the American Chemical Society, 1940 , vol. 62, p. 179
反应条件
1: m-chloroperbenzoic acid 2: 81 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C 3: 82 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C 4: 79 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating 5: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 81 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C 2: 82 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C 3: 79 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating 4: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 2: 62 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C 3: 79 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating 4: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 1.) lithium naphthalenide 2: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 1.) lithium naphthalenide / 1.) 2 h, 2.) TMEDA, room temperature 2: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 88 percent / m-chloroperbenzoic acid / CH2Cl2 / -23 °C 2: 82 percent / butyl-lithium / hexane; tetrahydrofuran / 0 °C 3: 79 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating 4: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 62 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C 2: 79 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating 3: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
