N-(1-苯基丙基)苯胺合成路线 (共 22 条)
反应条件
1: NaHCO3; 4 Angstroem molecular sieves / benzene / Heating 2: 97 percent / aq. 2-propanol / [Ru2(CO)4(μ-H)(C4Ph4COHOCC4Ph4)] / benzene / 1 h / 70 °C View Scheme
参考文献
Wang, Zhouyu; Wang, Chao; Zhou, Li; Sun, Jian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 5 p. 787 - 797
反应条件
1: NaHCO3; 4 Angstroem molecular sieves / benzene / Heating 2: 97 percent / aq. 2-propanol / [Ru2(CO)4(μ-H)(C4Ph4COHOCC4Ph4)] / benzene / 1 h / 70 °C View Scheme
参考文献
Wang, Zhouyu; Wang, Chao; Zhou, Li; Sun, Jian
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 5 p. 787 - 797
反应条件
1: ethyl bromide With magnesium in tetrahydrofuran T=50°C; 12 h; Inert atmosphereReflux; 2: N-benzylideneaniline With titanium(IV) isopropylate in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; 3: With ammonium chloride in tetrahydrofuran; water
参考文献
Kumar, Akshai; Samuelson, Ashoka G.
Chemistry - An Asian Journal, 2010 , vol. 5, # 8 p. 1830 - 1837
反应条件
in hexane; dichloromethane T=20°C; 0.0833333 h;
参考文献
Miyabe, Hideto; Yamaoka, Yousuke; Takemoto, Yoshiji
Journal of Organic Chemistry, 2006 , vol. 71, # 5 p. 2099 - 2106
反应条件
in diethyl ether; hexane T=20°C; 0.25 h;
参考文献
Miyata, Okiko; Ishikawa, Tatsuya; Ueda, Masafumi; Naito, Takeaki
Synlett, 2006 , # 14 p. 2219 - 2222
反应条件
potassium hydroxide; hydrazine hydrate; 1,2-bis-(2-hydroxyethoxy)-ethane
参考文献
Leonard; Gelfand
Journal of the American Chemical Society, 1955 , vol. 77, p. 3272,3274,3276
参考文献
Rosser; Ritter
Journal of the American Chemical Society, 1937 , vol. 59, p. 2179
反应条件
bis(η5-cyclopentadienyl)MoH2; toluene-4-sulfonic acid in methanol 24 h; Ambient temperature;
参考文献
Minato, Makoto; Fujiwara, Yutaka; Ito, Takashi
Chemistry Letters, 1995 , # 8 p. 647 - 648
反应条件
1: With C38H66N4O2Zr; triphenylmethylium tetrakis(pentafluorophenyl)borate in chlorobenzene T=120°C; 1 h; Inert atmosphereGlovebox; 2: With lithium aluminium tetrahydride in chlorobenzene T=0 - 60°C; 2 h; Inert atmosphereGlovebox;
参考文献
Sun, Qiu; Wang, Yaorong; Yuan, Dan; Yao, Yingming; Shen, Qi
Organometallics, 2014 , vol. 33, # 4 p. 994 - 1001
反应条件
neodymium (III) chloride in hexane; benzene T=20°C; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Tsvelikhovsky, Dmitry; Schumann, Herbert; Blum, Jochanan
Synthesis, 2006 , # 11 p. 1819 - 1822