3,3-二甲基-1,2-环氧丁烷合成路线 (共 8 条)
反应条件
aluminium trichloride
参考文献
Inoue,M. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 1873 - 1874
反应条件
potassium hydroxide in dimethyl sulfoxide T=100°C;
参考文献
Mischitz; Kroutil; Wandel; Faber
Tetrahedron Asymmetry, 1995 , vol. 6, # 6 p. 1261 - 1272
反应条件
2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; cyclohexane T=20°C; 15 h;
参考文献
Katritzky, Alan R.; Fang, Yunfeng; Prakash, Indra
Journal of the Indian Chemical Society, 2000 , vol. 77, # 11-12 p. 635 - 636
反应条件
N-bromosuccinmide in water
参考文献
Price,C.C. et al.
Journal of the American Chemical Society, 1972 , vol. 94, # 11 p. 3964 - 3971
反应条件
sodium hydroxide in water
参考文献
Bayer Aktiengesellschaft
Patent: US4339612 A1, 1982 ;
反应条件
in acetonitrile
T=100°C; 24 h;
参考文献
Day, Joanna K.; Baghurst, Rebecca E.; Strevens, Robert R.; Light, Mark E.; Hursthouse, Michael B.; Stengel, Bruno F.; Fallis, Ian A.; Aldridge, Simon
New Journal of Chemistry, 2007 , vol. 31, # 1 p. 135 - 142
反应条件
carbon disulfide; sodium hydrogensulfide in methanol
T=25 - 30°C; 3 h;
参考文献
Wu, Shao-Yong; Hirashima, Akinori; Takeya, Ryuko; Eto, Morifusa
Agricultural and Biological Chemistry, 1988 , vol. 52, # 11 p. 2911 - 2918
反应条件
thiourea in methanol
T=80°C; 12 h;
参考文献
ABBOTT LABORATORIES
Patent: US2008/153883 A1, 2008 ;
Location in patent: Page/Page column 20 ;
US 20080153883 A1