1-甲基-2-丙烯基氯化镁合成路线 （共 21 条）
反应条件
magnesium in diethyl ether
参考文献
Lehmkuhl,H. et al.
Justus Liebigs Annalen der Chemie, 1975 , p. 119 - 144
反应条件
in diethyl ether Heating;
参考文献
Ashcroft, Martyn R.; Bury, Adrian; Cooksey, Christopher J.; Davies, Alwyn G.; Gupta, B. Dass; et al.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 89 - 104
反应条件
in diethyl ether T=-5°C;
参考文献
Ashcroft, Martyn R.; Bury, Adrian; Cooksey, Christopher J.; Davies, Alwyn G.; Gupta, B. Dass; et al.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 89 - 104
反应条件
in dichloromethane 8 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ohno, Masatomi; Shimizu, Kazuo; Ishizaki, Kenichi; Sasaki, Tadashi; Eguchi, Shoji
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 729 - 733
反应条件
1,3-bis-(diphenylphosphino)propane; CoCl2 in tetrahydrofuran T=-40°C;
参考文献
Tsuji, Takashi; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2002 , vol. 41, # 21 p. 4137 - 4139
反应条件
bis(2-methoxyethoxy)aluminum hydride; palladium on activated charcoal 1) THF, -70 deg C, 20 min, 2) 20 deg C, 150 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Barboni, Luciano; Bartoli, Giuseppe; Marcantoni, Enrico; Petrini, Marino; Dalpozzo, Renato
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 7 p. 2133 - 2138
参考文献
Wadamoto, Manabu; Ozasa, Nobuko; Yanagisawa, Akira; Yamamoto, Hisashi
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5593 - 5601
反应条件
1: in tetrahydrofuran T=-60°C; 4 h; 2: With ammonium chloride
参考文献
BOEHRINGER INGELHEIM PHARMACEUTICALS, INC.
Patent: WO2005/30213 A1, 2005 ;
Location in patent: Page/Page column 195-196 ;
WO 2005/030213 A1
反应条件
copper(l) iodide in diethyl ether
T=-30°C; other solvents investigated; stereochemical outcome also investigated; Product distribution;
参考文献
Hosomi, Akira; Iguchi, Hirokazu; Sakurai, Hideki
Chemistry Letters, 1982 , p. 223 - 226
反应条件
in diethyl ether
T=-5°C;
参考文献
Ashcroft, Martyn R.; Bury, Adrian; Cooksey, Christopher J.; Davies, Alwyn G.; Gupta, B. Dass; et al.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 89 - 104
