(1,13-十四烷二)烯合成路线 （共 19 条）
反应条件
1: With magnesium; ethylene dibromide in tetrahydrofuran T=20°C; Inert atmosphere; 2: With phosphorus trichoride in tetrahydrofuran Inert atmosphereCooling;
参考文献
Nawara-Hultzsch, Agnieszka J.; Skopek, Katrin; Shima, Takanori; Barbasiewicz, Micha; Hess, Gisela D.; Skaper, Dirk; Gladysz, John A.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 3 p. 414 - 424
参考文献
Journal of the American Chemical Society, , vol. 81, p. 4737,4741
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <8>13, p. 61,65
反应条件
sodium methylate in methanol (electrolysis);
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2714 - 2721
反应条件
1.1: potassium tert-butylate / Inert atmosphere 2.1: magnesium; ethylene dibromide / tetrahydrofuran / 20 °C / Inert atmosphere 2.2: Inert atmosphere; Cooling View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 3 p. 414 - 424
反应条件
copper(l) iodide; sodium; lithium 1.) ether, -20 deg C, 2 h; 2.) ether, -30 deg C, 75 min, 3.) ether, -35 deg C, 2.5 h;; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 41, # 3 p. 627 - 634
反应条件
(i) Mg, THF, (ii) /BRN= 605308/; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 3893 - 3903
参考文献
US2004/116763 A1, ;
Page 4 ;
反应条件
(i) Mg, THF, (ii) /BRN= 605308/; Multistep reaction. Further byproducts given;
参考文献
Bulletin de la Societe Chimique de France, , p. 3893 - 3903
反应条件
2,2,4-trimethylpentane; tetradecafluorohexane; bromine T=20°C; 2 h; Irradiation;
参考文献
Matsubara, Hiroshi; Tsukida, Masaaki; Ishihara, Daisuke; Kuniyoshi, Kenji; Ryu, Ilhyong
Synlett, 2010 , # 13 p. 2014 - 2018
反应条件
9-borabicyclo[3.3.1]nonane dimer; dimethylsulfide borane complex Product distribution;
参考文献
Brown, Herbert C.; Pai, Ganesh G.; Naik, Ramachandra G.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1072 - 1078
