2,6-二甲基-苯甲酰氯合成路线 （共 23 条）
反应条件
2: ethanol; sodium-amalgam View Scheme
参考文献
Coops et al.
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 1109,1111
反应条件
1.1: sodium hydrogencarbonate / 2-methyl tetrahydrofuran; water / 0.5 h / Cooling 1.2: 3 h / 10 °C / Cooling 2.1: water; sodium hydroxide / 2-methyl tetrahydrofuran / 1 h / 25 - 28 °C View Scheme
参考文献
Chavez, Flavio; Kennedy, Nicole; Rawalpally, Thimma; Williamson, R. Thomas; Cleary, Thomas
Organic Process Research and Development, 2010 , vol. 14, # 3 p. 579 - 584
反应条件
triethylamine in dichloromethane 1 h;
参考文献
Collman, James P.; Brauman, John I.; Fitzgerald, Jeffrey P.; Hampton, Philip D.; Naruta, Yoshinori; et al.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3477 - 3486
反应条件
water T=10°C; solvolysis examined; var. solvents and ratio of ones; mechanism; ΔH(excit.), ΔS(excit.); KineticsThermodynamic dataProduct distribution;
参考文献
Bentkey, T. William; Harris, H. Carl; Koo, In Sun
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 783 - 790
反应条件
water in acetone T=-20°C; Rate constant;
参考文献
Ugi,I.; Beck,F.
Chemische Berichte, 1961 , vol. 94, p. 1839 - 1850
反应条件
water T=10°C; solvolysis examined; var. solvents and ratio of ones; mechanism; ΔH(excit.), ΔS(excit.); KineticsThermodynamic dataProduct distribution;
参考文献
Bentkey, T. William; Harris, H. Carl; Koo, In Sun
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 783 - 790
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Haering,M.
Helvetica Chimica Acta, 1960 , vol. 43, p. 104 - 113
反应条件
quinoline; sulfur; toluene T=130 - 140°C; Hydrogenation.Reagens 4: Palladium-Katalysator;
参考文献
Lock; Schmidt
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 140, p. 229,231
反应条件
T=130 - 140°C; Hydrogenation;
参考文献
Lock; Schmidt
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 140, p. 229,231
参考文献
Aventis Pharma Deutschland GmbH
Patent: US7005440 B1, 2006 ;
Location in patent: Page/Page column 150 ;
US 7005440 B1
