N,N,2-三甲基丙酰胺合成路线 （共 43 条）
反应条件
in chloroform 6 h; Ambient temperature; Product distribution;
参考文献
Ernst, Beat.; Winkler, Tammo.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3081 - 3084
反应条件
in N,N-dimethyl-formamide T=20°C; Equilibrium constant; Further Variations:Solvents;
参考文献
New Journal of Chemistry, , vol. 28, # 1 p. 145 - 152
反应条件
in chloroform 6 h; Ambient temperature; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 23 p. 3081 - 3084
参考文献
Buswell, Marina; Fleming, Ian; Ghosh, Usha; Mack, Stephen; Russell, Matthew; Clark, Barry P.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 20 p. 3006 - 3017
参考文献
Izzo; Safir
Journal of Organic Chemistry, 1959 , vol. 24, p. 701
反应条件
in acetonitrile T=-30.16°C; Inert atmospherePhotolysis;
参考文献
Alberti, Angelo; Grossi, Loris; MacCiantelli, Dante
Tetrahedron, 2012 , vol. 68, # 12 p. 2662 - 2670
参考文献
Hullot,P. et al.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 1098 - 1104
Full Text Show Details
Cuvigny,T. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1974 , vol. 278, p. 1105 - 1108
反应条件
water; ammonium chloride 1.) THF, -78 deg C, 1.5 h, 2.) -78 deg C to r.t.; Multistep reaction;
参考文献
Fleming, Ian; Mack, Stephen R.; Clark, Barry P.
Chemical Communications, 1998 , # 6 p. 713 - 714
反应条件
1: in toluene T=65°C; Schlenk techniqueInert atmosphere; 2: With bromine in toluene T=-78°C; 0.0333333 h; Schlenk techniqueInert atmosphere; 3: With water in toluene T=20°C; 1 h; Schlenk techniqueInert atmosphere; regioselective reaction;
参考文献
Kobeissi, Marwan; Cherry, Khalil; Jomaa, Wissam
Synthetic Communications, 2013 , vol. 43, # 21 p. 2955 - 2965
反应条件
1: 1.) n-BuLi, 2,2,6,6-tetramethylpiperidine / 1.) THF, HMPA, hexane, 0 deg C, 20 min, 2.) THF, HMPA, hexane, 10 deg C, 15 min and 45 deg C, 30 min 2: 47 percent / BF3*Et2O, borane-dimethyl sulfide / tetrahydrofuran / 0.5 h / 0 - 45 °C View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 12 p. 2787 - 2793
