N-(3-氯苯基)氨基甲酸乙酯合成路线 （共 9 条）
反应条件
pyridine T=0°C; 1 h;
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: EP1364945 A1, 2003 ;
Location in patent: Page/Page column 28 ;
反应条件
1: carbon dioxide; 3-chloro-aniline With 2-pyrrolidone electrogenerated base*Et4N(+) in acetonitrile T=20°C; Carboxylation; 1 h; 2: ethyl iodide in acetonitrile T=20°C; Esterification;
参考文献
Feroci, Marta; Inesi, Achille; Rossi, Leucio
Tetrahedron Letters, 2000 , vol. 41, # 6 p. 963 - 966
反应条件
sodium hydride in benzene 1.5 h; Heating;
参考文献
Angeles; Santillan; Martinez; Ramirez; Moreno; Salmon
Synthetic Communications, 1994 , vol. 24, # 17 p. 2441 - 2447
反应条件
pyridine; oxygen; iron; iodine; palladium dichloride T=180°C; P=30003 Torr; 1 h;
参考文献
Karpinska; Baran; Skupinska
Polish Journal of Chemistry, 2008 , vol. 82, # 5 p. 1105 - 1116
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>64, p. 332
参考文献
Bulletin de la Societe Chimique de France, , vol. <3>21, p. 956
反应条件
1: nitric acid
2: sulfuric acid / 130 °C
View Scheme
参考文献
de Monchy
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 141,149,156
反应条件
n-butyllithium in tetrahydrofuran
T=-78 - 20°C;
参考文献
Adibpour, Neda; Khalaj, Ali; Rajabalian, Saeed
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 1 p. 19 - 24
反应条件
1: nitric acid
2: sulfuric acid; nitric acid / Erwaermen des Reaktionsprodukts mit Schwefelsaeure
View Scheme
参考文献
de Monchy
Recueil des Travaux Chimiques des Pays-Bas, 1934 , vol. 53, p. 141,149,156
