2,6-二甲基苯基溴化镁合成路线 （共 31 条）
反应条件
iodine; magnesium in tetrahydrofuran Metallation; 0.5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 65, # 10 p. 3154 - 3159
反应条件
in tetrahydrofuran 3 h; Heating;
参考文献
Vinod; Hart
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 881 - 890
反应条件
2: lithium aluminium hydride, aluminium chloride View Scheme
参考文献
Bethell, Donald; Hare, Gerard J.; Kearney, Paul A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 684 - 691
反应条件
copper(I) bromide; lithium bromide in tetrahydrofuran T=20°C;
参考文献
Bottalico, Daniela; Fiandanese, Vito; Marchese, Giuseppe; Punzi, Angela
Synlett, 2007 , # 6 p. 974 - 976
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED
Patent: US2003/158419 A1, 2003 ;
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in tetrahydrofuran T=60°C; 20 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Tetrahedron, 2008 , vol. 64, # 11 p. 2537 - 2552
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in tetrahydrofuran T=20°C; 20 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Tetrahedron, 2008 , vol. 64, # 11 p. 2537 - 2552
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in tetrahydrofuran T=20°C; 20 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Angewandte Chemie - International Edition, 2006 , vol. 45, # 14 p. 2289 - 2292
反应条件
palladium diacetate in tetrahydrofuran T=60°C; 20 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Organic Letters, 2006 , vol. 8, # 22 p. 5057 - 5060
反应条件
palladium diacetate in tetrahydrofuran 20 h; Heating;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Tetrahedron, 2008 , vol. 64, # 11 p. 2537 - 2552
