反应条件
LiMe in tetrahydrofuran Ar-atmosphere; treatment of HC(SiMe3)3 (in THF) with LiMe (in Et2O), evapn. of Et2O, refluxing for 4 h, dropwise addn. to Hg-compd., refluxing for 3 h; addn. to ice-water, extn. into Et2O, drying (MgSO4), solvent removal, extn. into hot heptane, fractional crystn.;
参考文献
Al-Juaid, Salih S.; Eaborn, Colin; Lickiss, Paul D.; Smith, J. David; Tavakkoli, Kayumars; Webb, Alexander D.
Journal of Organometallic Chemistry, 1996 , vol. 510, # 1-2 p. 143 - 151
