反应条件
1.1: tert.-butyl lithium / diethyl ether; pentane / 1 h / -78 - 25 °C / |Inert atmosphere 1.2: 6 h / -78 - 25 °C / |Inert atmosphere 1.3: 16 h / 0 - 40 °C / |Inert atmosphere 2.1: tris (triphenylphosphine)rhodium(I) chloride / 1,4-dioxane / 3 h / 135 °C / |Inert atmosphere View Scheme
参考文献
Kuninobu, Yoichiro; Yamauchi, Kanae; Tamura, Naoya; Seiki, Takayuki; Takai, Kazuhiko
Angewandte Chemie - International Edition, 2013 , vol. 52, # 5 p. 1520 - 1522
Angew. Chem., 2013 , vol. 125, # 5 p. 1560 - 1562