2,2-二氯苯并[D][1,3]二氧杂环戊烯合成路线 （共 13 条）
反应条件
2,2'-azo-bisisobutyronitrile; chlorine in tetrachloromethane T=80 - 85°C; 3.5 h;
参考文献
Cambanis, Anton; Baeuml, Englbert; Mayr, Herbert
Synthesis, 1988 , # 12 p. 961
反应条件
phosphorus pentachloride
反应条件
ZnCl2*Et2O in dichloromethane 4.5 h; Yields of byproduct given;
参考文献
Mayr, Herbert; Brueggen, Uwe von der
Chemische Berichte, 1988 , vol. 121, p. 339 - 346
反应条件
hydroxide; methyllithium; dihydrogen peroxide 1.) THF, RT, 1 h, 2.) THF, RT; Yield given. Multistep reaction;
参考文献
Kawaguchi, Taihei; Ishidoya, Masahiro; Suzuki, Akira
Heterocycles, 1982 , vol. 18, p. 113 - 116
反应条件
hydroxide; methyllithium; dihydrogen peroxide multistep reaction; other organoborane, mechanism;
参考文献
Kawaguchi, Taihei; Ishidoya, Masahiro; Suzuki, Akira
Heterocycles, 1982 , vol. 18, p. 113 - 116
反应条件
hydroxide; methyllithium; dihydrogen peroxide 1.) THF, RT, 1 h, 2.) THF, RT; Yield given. Multistep reaction;
参考文献
Kawaguchi, Taihei; Ishidoya, Masahiro; Suzuki, Akira
Heterocycles, 1982 , vol. 18, p. 113 - 116
反应条件
hydroxide; methyllithium; dihydrogen peroxide 1.) THF, RT, 1 h, 2.) THF, RT; Yield given. Multistep reaction;
参考文献
Kawaguchi, Taihei; Ishidoya, Masahiro; Suzuki, Akira
Heterocycles, 1982 , vol. 18, p. 113 - 116
反应条件
(HF)10-pyridine T=20°C; 2 h;
参考文献
Saint-Jalmes, Laurent
Journal of Fluorine Chemistry, 2006 , vol. 127, # 1 p. 85 - 90
反应条件
potassium fluoride in 1.4-dicyano 1-butene
参考文献
FMC Corporation
Patent: US4895871 A1, 1990 ;
参考文献
Gross; Keitel; Costisella
Acta Chimica Hungarica, 1984 , vol. 116, # 3 p. 229 - 233
