2-偶氮基-3-氧代-1-苯基-1-丁烯-1-醇合成路线 （共 15 条）
反应条件
potassium fluoride; dibenzo-18-crown-6; 4-toluenesulfonyl azide in dichloromethane 1 h; Ambient temperature;
参考文献
Kitamura, Mitsuru; Tashiro, Norifumi; Miyagawa, Satoshi; Okauchi, Tatsuo
Synthesis, 2011 , # 7 p. 1037 - 1044
反应条件
triethylamine in tetrahydrofuran T=0°C; 0.166667 h;
参考文献
Kitamura, Mitsuru; Tashiro, Norifumi; Okauchi, Tatsuo
Synlett, 2009 , # 18 p. 2943 - 2944
参考文献
Minnesota Mining and Manufacturing Company
Patent: US5756689 A1, 1998 ;
反应条件
amalgamated zinc; sulfuric acid Behandlung des Reaktionsproduktes mit Natriumnitrit-Loesung;
参考文献
Wolff
Justus Liebigs Annalen der Chemie, 1902 , vol. 325, p. 137
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 46 Anm. 2
反应条件
nachf. Diazotierung mit Natriumnitrit;
参考文献
Wolff
Justus Liebigs Annalen der Chemie, 1902 , vol. 325, p. 137
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 46 Anm. 2
反应条件
in acetonitrile 4.75 h; Irradiation; Yields of byproduct given;
参考文献
Sauers, R. R.; Hadel, L. M.; Scimone, A. A.; Stevenson, T. A.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4011 - 4019
参考文献
Justus Liebigs Annalen der Chemie, , vol. 325, p. 137
Justus Liebigs Annalen der Chemie, , vol. 394, p. 46 Anm. 2
反应条件
1: diethyl ether 2: diluted alcohol View Scheme
参考文献
Staudinger; Luescher
Helvetica Chimica Acta, 1922 , vol. 5, p. 84
反应条件
in 1,4-dioxane T=10°C; Irradiationalso thermolysis at 80 deg C, other 2-diazo-1,3-dicarbonyl compounds; Product distributionMechanism;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 3 p. 758 - 761
反应条件
aluminum oxide in diethyl ether; pentane
参考文献
Korneev; Richter
Synthesis, 1995 , # 10 p. 1248 - 1250
