4-甲基-2-苯基苯乙酮合成路线 (共 107 条)
反应条件
aluminium trichloride T=20°C;
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 10 p. 1870 - 1877
反应条件
ammonium chloride; bipyridine-cyclopalladated ferrocenylimine complex in water T=100°C; 24 h;
参考文献
Synlett, , # 19 p. 3063 - 3067
反应条件
pyridine; 1,10-phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide in 1-methyl-pyrrolidin-2-one T=170°C; 36 h;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 16 p. 3043 - 3045
反应条件
1: With sodium hydrogencarbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=150°C; Heck reaction; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=25°C; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3122 - 3132
反应条件
palladium diacetate; 1,4-di(diphenylphosphino)-butane in tetrahydrofuran T=90°C; P=1500.15 Torr; 1 h; Sealed tubeMicrowave irradiation; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 22 p. 4729 - 4733
反应条件
PdCl2bis(phenylimino)acenaphthene; fumaric acid dimethyl ester in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; P=825.07 Torr; 15 h;
参考文献
Tetrahedron, , vol. 50, # 2 p. 323 - 334
反应条件
phosphoric acid; trifluoroacetic anhydride T=25°C; 0.0166667 h;
参考文献
Medicinal Chemistry Research, , vol. 21, # 7 p. 1313 - 1321
反应条件
water; toluene-4-sulfonic acid in ethanol T=150°C; 0.5 h; Microwave irradiation; regioselective reaction;
参考文献
Tetrahedron, , vol. 66, # 21 p. 3775 - 3787
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene; [(t-Bu)3PH]BF4 in tetrahydrofuran T=120°C; P=2250.23 Torr; 0.5 h; Microwave irradiationSealed tube; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 22 p. 4729 - 4733
反应条件
lithium bromide in diethyl ether T=0°C;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 90, # 9 p. 985 - 986