1: in tetrahydrofuran T=0 - 20°C; Weinreb ketone synthesis; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water pH=2; Inert atmosphere;
1: vinyl-magnesium bromide With indium(III) chloride in tetrahydrofuran 2: benzoyl chloride With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 1 h;
参考文献
Lee, Phil Ho; Lee, Sung Wook; Seomoon, Dong
Organic Letters, 2003 , vol. 5, # 26 p. 4963 - 4966