1,2-二氢-2-氰基喹啉-1-羧酸乙酯合成路线 （共 15 条）
反应条件
in dichloromethane; water T=20°C; 2 h;
参考文献
Kim, Sung Hwan; Kim, Yu Mi; Park, Bo Ram; Kim, Jae Nyoung
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 3031 - 3034
反应条件
iodine in dichloromethane T=20°C; 3 h;
参考文献
Yadav; Reddy; Srinivas; Sathaiah
Tetrahedron Letters, 2005 , vol. 46, # 20 p. 3489 - 3492
反应条件
1: CH2Cl2 / 0.5 h / 20 °C 2: iodine / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Yadav; Reddy; Srinivas; Sathaiah
Tetrahedron Letters, 2005 , vol. 46, # 20 p. 3489 - 3492
反应条件
potassium cyanide in dichloromethane; water 3 h;
参考文献
Cremin, Denis J.; Hegarty, Anthony F.; Begley, Michael J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 412 - 420
反应条件
1: Irradiation 2: K2CO3 / methanol / 0 °C View Scheme
参考文献
Takeda; Shudo; Okamoto; Kosuge
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1280 - 1285
反应条件
1: Irradiation 2: 90 percent / LDA / tetrahydrofuran / -78 deg C, 5 min, RT 3: 84 percent / potassium carbonate / methanol / 0.92 h / Ambient temperature 4: 23 percent / aluminum chloride / 12 h / 100 - 120 °C View Scheme
参考文献
Takeda; Shudo; Okamoto; Kosuge
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1280 - 1285
反应条件
1: Irradiation 2: K2CO3 / methanol / 0 °C 3: 24 percent / aluminum chloride / 12 h / 100 - 120 °C View Scheme
参考文献
Takeda; Shudo; Okamoto; Kosuge
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1280 - 1285
反应条件
sodium hydroxide; oxygen; benzyltriethylammonium hydroxide in water; benzene Ambient temperature;
参考文献
Rozwadowska, Maria; Brozda, Danuta
Canadian Journal of Chemistry, 1980 , vol. 58, p. 1239 - 1242
反应条件
1: Irradiation
2: K2CO3 / methanol / 0 °C
3: 29 percent / aluminum chloride / 12 h / 100 - 120 °C
View Scheme
参考文献
Takeda; Shudo; Okamoto; Kosuge
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1280 - 1285
反应条件
1: Irradiation
2: K2CO3 / methanol / 0 °C
3: 10 percent / aluminum chloride / 12 h / 100 - 120 °C
View Scheme
参考文献
Takeda; Shudo; Okamoto; Kosuge
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1280 - 1285
