三甲基-(4-甲基苯氧基)硅烷合成路线 (共 16 条)
反应条件
1,3-disulfonic acid imidazolium hydrogen sulfate in neat (no solvent) T=20°C; 0.0166667 h; Green chemistry;
参考文献
Shirini, Farhad; Khaligh, Nader Ghaffari; Akbari-Dadamahaleh, Somayeh
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 365, p. 15 - 23
反应条件
lithium perchlorate; silica gel in dichloromethane T=20°C; 2 h;
参考文献
Azizi, Najmedin; Yousefi, Rozbeh; Saidi, Mohammad R.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 5 p. 817 - 820
反应条件
in pyridine T=115°C; 3 h;
参考文献
Felpin, Francois-Xavier
Tetrahedron Letters, 2007 , vol. 48, # 3 p. 409 - 412
反应条件
Fe(ClO4)3*6H2O in dichloromethane T=20°C; 3 h;
参考文献
Oskooie, Hossein A.; Heravi, Majid M.; Tehrani, Maryam H.; Behbahani, Farahnaz K.; Heravi, Omid M.
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 7 p. 1729 - 1737
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=20°C; 3.5 h;
参考文献
Iida, Akira; Horii, Atsushi; Misaki, Tomonori; Tanabe, Yoo
Synthesis, 2005 , # 16 art. no. F06305SS, p. 2677 - 2682
反应条件
in dichloromethane T=40°C; 2 h;
参考文献
Verboom, W.; Visser, G. W.; Reinhoudt, D. N.
Synthesis, 1981 , # 10 p. 807 - 809
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 7 h; Ambient temperature;
参考文献
Nakamura, Eiichi; Hashimoto, Koichi; Kuwajima, Isao
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 805 - 808
反应条件
1: 95 percent / imidazole / dimethylformamide / 1 h / 40 °C 2: <CH3(CH2)3>4NF / tetrahydrofuran / 20 °C / other reaction partners (HCl, KPF6, CF3COOH, BF3), other solvent (ether), other reaction times 3: 95 percent / 12 h / 30 °C View Scheme
参考文献
Giral, L.; Madit, N.; Montginoul, C.; Sagnes, R.; Schue, F.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 147 - 166
反应条件
1: <CH3(CH2)3>4NF / tetrahydrofuran / 20 °C / other reaction partners (HCl, KPF6, CF3COOH, BF3), other solvent (ether), other reaction times 2: 95 percent / 12 h / 30 °C View Scheme
参考文献
Giral, L.; Madit, N.; Montginoul, C.; Sagnes, R.; Schue, F.
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 3 p. 147 - 166
参考文献
Jung,M.E.; Lyster,M.A.
Journal of Organic Chemistry, 1977 , vol. 42, p. 3761 - 3764