4-甲氧基苯甲醛2,4-二硝基苯基腙合成路线 (共 11 条)
反应条件
1: (4-methoxyphenyl)methanol With 3,6-bis(triphenylphosphonium)cyclohexene dichromate T=20°C; 0.0833333 h; 2: (2,4-dinitro-phenyl)-hydrazine 0.416667 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 182, # 3 p. 601 - 605
反应条件
sulfuric acid; silica gel 0.15 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 179, # 3 p. 569 - 573
反应条件
iron (III) perchlorate in 1,2-dichloro-ethane T=20°C; 24 h;
参考文献
Mendeleev Communications, , vol. 17, # 3 p. 190 - 191
反应条件
1: (diacetoxyiodo)benzene / RuCl3 / acetonitrile; H2O / 0.5 h / 20 °C 2: H2SO4 / acetonitrile; H2O; ethanol View Scheme
参考文献
Tetrahedron Letters, , vol. 47, # 35 p. 6305 - 6308
反应条件
1: 4-methoxy-benzylamine With cyclohepta[b]pyrimido[5,4-d]furan-8(7H),10(9H)-dionylium ion in acetonitrile 16 h; Irradiation; 2: (2,4-dinitro-phenyl)-hydrazine With hydrogenchloride in diethyl ether; water
参考文献
Tetrahedron, , vol. 60, # 41 p. 9139 - 9148
反应条件
1: N-chlorosuccinimide / H2O / 24.9 °C / pH 10.6; ΔH(excit.), ΔS(excit.) 2: 2 M HCl View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1015 - 1020
反应条件
1: NaOMe / methanol 2: (i) aq. NaOH, MeOH, (ii) /BRN= 615586/, H2SO4 View Scheme
参考文献
Indian Journal of Chemistry, , vol. 9, p. 658 - 659
参考文献
Gazzetta Chimica Italiana, , vol. 58, p. 385,388,390
Gazzetta Chimica Italiana, , vol. 59, p. 606
反应条件
1: aq.-ethanolic ammonia; hydrazine hydrate View Scheme
参考文献
Journal of the Chemical Society, , p. 756,758
参考文献
Journal of the Chemical Society, , p. 369