1,4-二氧螺环[4,5]癸烷合成路线 （共 57 条）
反应条件
N,N,N',N,-tetramethylethylenediamine in hexane 1.5 h;
参考文献
Ho, Tse-Lok
Synthetic Communications, 1983 , vol. 13, # 9 p. 769 - 772
反应条件
tetrachlorosilane; KU-2 (H+) cation exchange resin T=100°C; 4 h; other chlorosilane reagent; Product distribution;
参考文献
Mullakhmetova, Z. F.; Nedogrei, E. P.; Musavirov, R. S.; Kantor, E. A.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 1 p. 229 - 230,205 - 206
反应条件
1,1,1-trifluoropropanone; methyl(trifluoromethyl)dioxirane in dichloromethane T=0°C; 2 h; also dimethyldioxirane efficiently afford cleavage of acetals and ketals to carbonyl products under mild, neutral conditions through α-CH insertion, also react dialkyl ethers and cyclic ethers to alcohols, aldehydes, carboxylic axids or to lactones;
参考文献
Curci; D'Accolti; Fiorentino; Fusco; Adam; Gonzalez-Nunez; Mello
Tetrahedron Letters, 1992 , vol. 33, # 29 p. 4225 - 4228
反应条件
chlorine dioxide in acetonitrile T=35°C; 12 h; Kinetics; Further Variations:TemperaturesSolvents;
参考文献
Russian Chemical Bulletin, , vol. 53, # 8 p. 1755 - 1760
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
iodine in chloroform T=20°C; 0.666667 h;
参考文献
Firouzabadi; Iranpoor; Hazarkhani
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7527 - 7529
反应条件
acetyl chloride in methanol 0.6 h; RefluxGreen chemistry; TemperatureTime; chemoselective reaction;
参考文献
Yu, Hai-Feng
Synthetic Communications, 2013 , vol. 43, # 9 p. 1280 - 1286
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
