5 5'-二甲基-2,2'-二吡啶合成路线 (共 36 条)
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Tetrahedron, , vol. 68, # 10 p. 2383 - 2390
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=110°C; Stille cross-coupling; 18 h;
参考文献
Verniest, Guido; Wang, Xingpo; De Kimpe, Norbert; Padwa, Albert
Journal of Organic Chemistry, 2010 , vol. 75, # 2 p. 424 - 433
反应条件
potassium phosphate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=100°C;
参考文献
Tetrahedron Letters, , vol. 44, # 14 p. 2935 - 2938
反应条件
iron(III) chloride T=330°C;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
1: phosphorus (III)-bromide / 190 °C 2: copper View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
1: copper-powder / 300 °C 2: phosphorus (III)-bromide / 190 °C 3: copper View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
1: aqueous NH3 / 120 - 140 °C 2: copper-powder / 300 °C 3: phosphorus (III)-bromide / 190 °C 4: copper View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2574,2576
反应条件
tert-butylaminotris(dimethylamino)phosphazene (phosphazene base P1-t-Bu) in methanol-d4; dichloromethane-d2 T=24.84°C; 2 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 49, # 94 p. 11077 - 11079