1: alpha-(bromomethyl)-acrylic acid With thionyl chloride T=60°C; 1.5 h; 2: ethanol T=20°C; 2 h; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of the Chinese Chemical Society, , vol. 55, # 2 p. 435 - 438
1: (4-bromophenyl)dichloroborane With i -Pr2Zn in diethyl ether T=25°C; 2 h; 2: in tetrahydrofuran T=-30°C; 0.166667 h; 3: 2-(bromomethyl)propenoic acid ethyl ester in tetrahydrofuran T=20°C; Further stages.;
参考文献
Hupe, Eike; Calaza, M. Isabel; Knochel, Paul
Chemical Communications, 2002 , # 13 p. 1390 - 1391
