1-苯基-3-丁炔-1-醇合成路线 （共 77 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide T=0 - 20°C; silylation;
参考文献
Marshall, James A.; Yanik, Mathew M.
Organic Letters, 2000 , vol. 2, # 14 p. 2173 - 2175
反应条件
1: periodic acid; pyridinium chlorochromate / acetonitrile / 0 °C / |Inert atmosphere 2: gold(III) chloride; sodium carbonate; TIPS-EBX / isopropyl alcohol / 72 h / 23 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 26 p. 6743 - 6747
反应条件
1: periodic acid; pyridinium chlorochromate / acetonitrile / 0 °C / |Inert atmosphere 2: dichloro(2-pyridinecarboxylato)gold / acetonitrile / 72 h / 23 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 26 p. 6743 - 6747
反应条件
sulfuric acid in acetic acid 6 h;
参考文献
Synthetic Communications, , vol. 10, # 8 p. 637 - 644
参考文献
Synthetic Communications, , vol. 10, # 8 p. 637 - 644
反应条件
[Ru(N,N-bis[(pyridin-2-yl)methyl][2-(diphenylphosphino)phenyl]methanamine)(CH3COO)][BPh4] in tetrahydrofuran T=80°C; 17 h; Inert atmosphere;
参考文献
Liu, Fei Nian; Su, Fu Hai; Wen, Ting Bin; Sung, Herman H.-Y.; Williams, Ian D.; Jia, Guochen
Chemistry - A European Journal, 2010 , vol. 16, # 26 p. 7889 - 7897
反应条件
hydrogen; palladium on activated charcoal Title compound not separated from byproducts;
参考文献
Haruta, Ryuichi; Ishiguro, Masaharu; Ikeda, Nobuo; Yamamoto, Hisashi
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7667 - 7669
反应条件
hydrogen; palladium on activated charcoal Title compound not separated from byproducts;
参考文献
Haruta, Ryuichi; Ishiguro, Masaharu; Ikeda, Nobuo; Yamamoto, Hisashi
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7667 - 7669
反应条件
1,2-di-iodoethane; zinc in tetrahydrofuran
Barbier-type reaction; 2.5 h; sonochemical reaction;
参考文献
Lee, Adam Shih-Yuan; Chu, Shu-Fang; Chang, Yu-Ting; Wang, Shu-Huei
Tetrahedron Letters, 2004 , vol. 45, # 7 p. 1551 - 1553
反应条件
in diethyl ether
T=0 - 20°C; Inert atmosphere;
参考文献
Maraval, Valerie; Duhayon, Carine; Coppel, Yannick; Chauvin, Remi
European Journal of Organic Chemistry, 2008 , # 30 p. 5144 - 5156
